Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine

Idha Royani; Jumatul Rahmayani; Maimuna; Erry Koriyanti; Jorena; Khairul Saleh; Fiber Monado

doi:10.4028/www.scientific.net/KEM.860.297

Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine

Idha Royani^*
, Jumatul Rahmayani
, Maimuna
, Erry Koriyanti
, Jorena
, Khairul Saleh
, Fiber Monado

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Scopus citations

Abstract

The extraction process is a crucial part of the synthesis of Molecularly Imprinted Polymers (MIP). The process will have a significant impact on the number of its cavities that affects the polymers’ ability to recognize targets with the same physical and chemical properties as the analytes. Caffeine polymers have been prepared by the cooling-heating method using methacrylic acid (MAA) as a monomer, ethylene glycol dimethacrylate (EDMA) as a crosslinker, benzoyl peroxide (BPO) as an initiator, and chloroform as a solvent. The resulting caffeine polymer powder was extracted using chloroform, methanol / acetic acid (1:20), and methanol, respectively. Finally, the polymer powder is washed using the aquabidest, which is heated at 60°C. The results of FTIR, XRD, and SEM characterization showed that caffeine concentration was significantly reduced. The number of cavities obtained from caffeine MIP is 604 more than before extracted, which is 132 pieces.

Original language	English
Title of host publication	Physics Symposium
Subtitle of host publication	Key Research in Materials Science
Editors	Ayi Bahtiar, Togar Saragi, Sahrul Hidayat, Lusi Safriani
Publisher	Trans Tech Publications Ltd
Pages	297-302
Number of pages	6
ISBN (Print)	9783035716979
DOIs	https://doi.org/10.4028/www.scientific.net/KEM.860.297
State	Published - 2020
Externally published	Yes
Event	4th Padjadjaran International Physics Symposium, PIPS 2019 - Bandung, Indonesia Duration: 13 Nov 2019 → 14 Nov 2019

Publication series

Name	Key Engineering Materials
Volume	860 KEM
ISSN (Print)	1013-9826
ISSN (Electronic)	1662-9795

Conference

Conference	4th Padjadjaran International Physics Symposium, PIPS 2019
Country/Territory	Indonesia
City	Bandung
Period	13/11/19 → 14/11/19

Bibliographical note

Publisher Copyright:
© 2020 Trans Tech Publications Ltd, Switzerland.

Keywords

Cavities
Cooling-heating
Extraction
MIP caffeine
Polymer

ASJC Scopus subject areas

General Materials Science
Mechanics of Materials
Mechanical Engineering

Access to Document

10.4028/www.scientific.net/KEM.860.297

Cite this

Royani, I., Rahmayani, J., Maimuna, Koriyanti, E., Jorena, Saleh, K., & Monado, F. (2020). Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine. In A. Bahtiar, T. Saragi, S. Hidayat, & L. Safriani (Eds.), Physics Symposium: Key Research in Materials Science (pp. 297-302). (Key Engineering Materials; Vol. 860 KEM). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/KEM.860.297

Royani, Idha ; Rahmayani, Jumatul ; Maimuna et al. / Temperature in the extraction process : The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine. Physics Symposium: Key Research in Materials Science. editor / Ayi Bahtiar ; Togar Saragi ; Sahrul Hidayat ; Lusi Safriani. Trans Tech Publications Ltd, 2020. pp. 297-302 (Key Engineering Materials).

@inproceedings{b0ec30eb01534b62b1cfcae65dedcf58,

title = "Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine",

abstract = "The extraction process is a crucial part of the synthesis of Molecularly Imprinted Polymers (MIP). The process will have a significant impact on the number of its cavities that affects the polymers{\textquoteright} ability to recognize targets with the same physical and chemical properties as the analytes. Caffeine polymers have been prepared by the cooling-heating method using methacrylic acid (MAA) as a monomer, ethylene glycol dimethacrylate (EDMA) as a crosslinker, benzoyl peroxide (BPO) as an initiator, and chloroform as a solvent. The resulting caffeine polymer powder was extracted using chloroform, methanol / acetic acid (1:20), and methanol, respectively. Finally, the polymer powder is washed using the aquabidest, which is heated at 60°C. The results of FTIR, XRD, and SEM characterization showed that caffeine concentration was significantly reduced. The number of cavities obtained from caffeine MIP is 604 more than before extracted, which is 132 pieces.",

keywords = "Cavities, Cooling-heating, Extraction, MIP caffeine, Polymer",

author = "Idha Royani and Jumatul Rahmayani and Maimuna and Erry Koriyanti and Jorena and Khairul Saleh and Fiber Monado",

note = "Publisher Copyright: {\textcopyright} 2020 Trans Tech Publications Ltd, Switzerland.; 4th Padjadjaran International Physics Symposium, PIPS 2019 ; Conference date: 13-11-2019 Through 14-11-2019",

year = "2020",

doi = "10.4028/www.scientific.net/KEM.860.297",

language = "English",

isbn = "9783035716979",

series = "Key Engineering Materials",

publisher = "Trans Tech Publications Ltd",

pages = "297--302",

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Royani, I, Rahmayani, J, Maimuna, Koriyanti, E, Jorena, Saleh, K & Monado, F 2020, Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine. in A Bahtiar, T Saragi, S Hidayat & L Safriani (eds), Physics Symposium: Key Research in Materials Science. Key Engineering Materials, vol. 860 KEM, Trans Tech Publications Ltd, pp. 297-302, 4th Padjadjaran International Physics Symposium, PIPS 2019, Bandung, Indonesia, 13/11/19. https://doi.org/10.4028/www.scientific.net/KEM.860.297

Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine. / Royani, Idha; Rahmayani, Jumatul; Maimuna et al.
Physics Symposium: Key Research in Materials Science. ed. / Ayi Bahtiar; Togar Saragi; Sahrul Hidayat; Lusi Safriani. Trans Tech Publications Ltd, 2020. p. 297-302 (Key Engineering Materials; Vol. 860 KEM).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AU - Royani, Idha

AU - Rahmayani, Jumatul

AU - Maimuna,

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AU - Jorena,

AU - Saleh, Khairul

AU - Monado, Fiber

PY - 2020

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N2 - The extraction process is a crucial part of the synthesis of Molecularly Imprinted Polymers (MIP). The process will have a significant impact on the number of its cavities that affects the polymers’ ability to recognize targets with the same physical and chemical properties as the analytes. Caffeine polymers have been prepared by the cooling-heating method using methacrylic acid (MAA) as a monomer, ethylene glycol dimethacrylate (EDMA) as a crosslinker, benzoyl peroxide (BPO) as an initiator, and chloroform as a solvent. The resulting caffeine polymer powder was extracted using chloroform, methanol / acetic acid (1:20), and methanol, respectively. Finally, the polymer powder is washed using the aquabidest, which is heated at 60°C. The results of FTIR, XRD, and SEM characterization showed that caffeine concentration was significantly reduced. The number of cavities obtained from caffeine MIP is 604 more than before extracted, which is 132 pieces.

AB - The extraction process is a crucial part of the synthesis of Molecularly Imprinted Polymers (MIP). The process will have a significant impact on the number of its cavities that affects the polymers’ ability to recognize targets with the same physical and chemical properties as the analytes. Caffeine polymers have been prepared by the cooling-heating method using methacrylic acid (MAA) as a monomer, ethylene glycol dimethacrylate (EDMA) as a crosslinker, benzoyl peroxide (BPO) as an initiator, and chloroform as a solvent. The resulting caffeine polymer powder was extracted using chloroform, methanol / acetic acid (1:20), and methanol, respectively. Finally, the polymer powder is washed using the aquabidest, which is heated at 60°C. The results of FTIR, XRD, and SEM characterization showed that caffeine concentration was significantly reduced. The number of cavities obtained from caffeine MIP is 604 more than before extracted, which is 132 pieces.

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KW - Extraction

KW - MIP caffeine

KW - Polymer

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M3 - Conference contribution

AN - SCOPUS:85091331359

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PB - Trans Tech Publications Ltd

Y2 - 13 November 2019 through 14 November 2019

ER -

Royani I, Rahmayani J, Maimuna, Koriyanti E, Jorena, Saleh K et al. Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine. In Bahtiar A, Saragi T, Hidayat S, Safriani L, editors, Physics Symposium: Key Research in Materials Science. Trans Tech Publications Ltd. 2020. p. 297-302. (Key Engineering Materials). doi: 10.4028/www.scientific.net/KEM.860.297

Temperature in the extraction process: The number of cavities created in polymer based on molecularly imprinted polymer (mip) caffeine

Abstract

Publication series

Conference

Bibliographical note

Keywords

ASJC Scopus subject areas

Access to Document

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Cite this