SYNTHESIS OF FACETTED GAMMA ALUMINA NANOPARTICLES FROM WASTE BEVERAGE ALUMINIUM CANS FOR POTENTIAL CATALYST SUPPORT APPLICATIONS

Rozita Yahaya; Ismail Zainol; Anwar Ul-Hamid; Hasliza Bahruji; Raja Mazuir Raja Ahsan Shah; Muhammad Hafiz Jasinih Jasri; Radiah Salleh

SYNTHESIS OF FACETTED GAMMA ALUMINA NANOPARTICLES FROM WASTE BEVERAGE ALUMINIUM CANS FOR POTENTIAL CATALYST SUPPORT APPLICATIONS

Rozita Yahaya^*
, Ismail Zainol
, Anwar Ul-Hamid
, Hasliza Bahruji
, Raja Mazuir Raja Ahsan Shah
, Muhammad Hafiz Jasinih Jasri
, Radiah Salleh

^*Corresponding author for this work

Core Research Facilities

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000^oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m²/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.

Original language	English
Pages (from-to)	78-87
Number of pages	10
Journal	Malaysian Journal of Microscopy
Volume	17
Issue number	2
State	Published - 20 Dec 2021

Bibliographical note

Publisher Copyright:
© Malaysian Journal of Microscopy (2021). All rights reserved.

Keywords

Green synthesis
TEM
XRD
waste aluminium cans
γ-Al2O3 nanoparticles

ASJC Scopus subject areas

Pathology and Forensic Medicine
Histology
Instrumentation

Cite this

@article{04d18738539e432ba85db6ddc563eec0,

title = "SYNTHESIS OF FACETTED GAMMA ALUMINA NANOPARTICLES FROM WASTE BEVERAGE ALUMINIUM CANS FOR POTENTIAL CATALYST SUPPORT APPLICATIONS",

abstract = "Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.",

keywords = "Green synthesis, TEM, XRD, waste aluminium cans, γ-Al2O3 nanoparticles",

author = "Rozita Yahaya and Ismail Zainol and Anwar Ul-Hamid and Hasliza Bahruji and Shah, \{Raja Mazuir Raja Ahsan\} and \{Jasinih Jasri\}, \{Muhammad Hafiz\} and Radiah Salleh",

year = "2021",

month = dec,

day = "20",

language = "English",

volume = "17",

pages = "78--87",

journal = "Malaysian Journal of Microscopy",

issn = "1823-7010",

publisher = "Microscopy Society of Malaysia",

number = "2",

}

TY - JOUR

T1 - SYNTHESIS OF FACETTED GAMMA ALUMINA NANOPARTICLES FROM WASTE BEVERAGE ALUMINIUM CANS FOR POTENTIAL CATALYST SUPPORT APPLICATIONS

AU - Yahaya, Rozita

AU - Zainol, Ismail

AU - Ul-Hamid, Anwar

AU - Bahruji, Hasliza

AU - Shah, Raja Mazuir Raja Ahsan

AU - Jasinih Jasri, Muhammad Hafiz

AU - Salleh, Radiah

PY - 2021/12/20

Y1 - 2021/12/20

N2 - Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.

AB - Green synthesis of gamma alumina (γ-Al2O3) nanoparticles (NPs) with facetted and cubeoctahedral morphologies was undertaken from waste (beverage aluminium cans) via precipitation technique and calcination at the temperature of 1000oC. The structural properties of γ-Al2O3 were determined with a combination of techniques including BET surface area, field emission scanning electron microscopy (FESEM) with energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM) and x-ray powder diffraction (XRD). XRD analysis confirmed the formation of γ-Al2O3 NPs by comparing with the standard of γ-Al2O3 structure. The BET surface area measured was 129 m2/g. High-resolution transmission electron microscopy (HRTEM) analysis provided evidence of surface-enhanced contrast in facetted γ-Al2O3 NPs structures similar to the commercial γ-Al2O3 NPs.

KW - Green synthesis

KW - TEM

KW - XRD

KW - waste aluminium cans

KW - γ-Al2O3 nanoparticles

UR - https://www.scopus.com/pages/publications/85127778356

M3 - Article

AN - SCOPUS:85127778356

SN - 1823-7010

VL - 17

SP - 78

EP - 87

JO - Malaysian Journal of Microscopy

JF - Malaysian Journal of Microscopy

IS - 2

ER -

SYNTHESIS OF FACETTED GAMMA ALUMINA NANOPARTICLES FROM WASTE BEVERAGE ALUMINIUM CANS FOR POTENTIAL CATALYST SUPPORT APPLICATIONS

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

Fingerprint

Cite this