Synthesis and optical properties of CuO nanostructures obtained via a novel thermal decomposition method

R. Al-Gaashani; S. Radiman; N. Tabet; A. Razak Daud

doi:10.1016/j.jallcom.2011.06.056

Synthesis and optical properties of CuO nanostructures obtained via a novel thermal decomposition method

R. Al-Gaashani^*, S. Radiman, N. Tabet, A. Razak Daud

^*Corresponding author for this work

King Fahd University of Petroleum & Minerals

Research output: Contribution to journal › Article › peer-review

113 Scopus citations

Abstract

We report a novel method that allows the synthesis of copper oxide (CuO) nanostructures and control their morphology and size by rapid thermal decomposition of copper nitrate (CuN₂O₆) under ambient conditions. The size and morphology of the nanostructures can be controlled by changing the temperature and the duration of the decomposition process. The structure of the products was investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS). The results showed that the morphology of the nanostructures changed as the temperature was varied and their size increased with increasing the treatment time. The optical properties of the samples were investigated by UV-vis spectroscopy and a photoluminescence (PL) spectrometer. Rice-like nanostructures were observed and analyzed by X-ray photoelectron spectroscopy (XPS)/EDS and XRD which confirmed that the as-synthesized powders correspond to pure CuO.

Original language	English
Pages (from-to)	8761-8769
Number of pages	9
Journal	Journal of Alloys and Compounds
Volume	509
Issue number	35
DOIs	https://doi.org/10.1016/j.jallcom.2011.06.056
State	Published - 1 Sep 2011

Bibliographical note

Funding Information:
The authors would like to thank Universiti Kebangsaan Malaysia (UKM) for supporting this work through grant no: UKM-GUP-NBT-08-27-106 and UKM-AP-NBT-15-2010 .

Keywords

CuO
Nanostructures
Optical properties
Thermal decomposition

ASJC Scopus subject areas

Mechanics of Materials
Mechanical Engineering
Metals and Alloys
Materials Chemistry

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10.1016/j.jallcom.2011.06.056

Cite this

@article{64ba726ab0f149d39a1e103c47891058,

title = "Synthesis and optical properties of CuO nanostructures obtained via a novel thermal decomposition method",

abstract = "We report a novel method that allows the synthesis of copper oxide (CuO) nanostructures and control their morphology and size by rapid thermal decomposition of copper nitrate (CuN2O6) under ambient conditions. The size and morphology of the nanostructures can be controlled by changing the temperature and the duration of the decomposition process. The structure of the products was investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS). The results showed that the morphology of the nanostructures changed as the temperature was varied and their size increased with increasing the treatment time. The optical properties of the samples were investigated by UV-vis spectroscopy and a photoluminescence (PL) spectrometer. Rice-like nanostructures were observed and analyzed by X-ray photoelectron spectroscopy (XPS)/EDS and XRD which confirmed that the as-synthesized powders correspond to pure CuO.",

keywords = "CuO, Nanostructures, Optical properties, Thermal decomposition",

author = "R. Al-Gaashani and S. Radiman and N. Tabet and \{Razak Daud\}, A.",

note = "Funding Information: The authors would like to thank Universiti Kebangsaan Malaysia (UKM) for supporting this work through grant no: UKM-GUP-NBT-08-27-106 and UKM-AP-NBT-15-2010 .",

year = "2011",

month = sep,

day = "1",

doi = "10.1016/j.jallcom.2011.06.056",

language = "English",

volume = "509",

pages = "8761--8769",

journal = "Journal of Alloys and Compounds",

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TY - JOUR

T1 - Synthesis and optical properties of CuO nanostructures obtained via a novel thermal decomposition method

AU - Al-Gaashani, R.

AU - Radiman, S.

AU - Tabet, N.

AU - Razak Daud, A.

N1 - Funding Information: The authors would like to thank Universiti Kebangsaan Malaysia (UKM) for supporting this work through grant no: UKM-GUP-NBT-08-27-106 and UKM-AP-NBT-15-2010 .

PY - 2011/9/1

Y1 - 2011/9/1

N2 - We report a novel method that allows the synthesis of copper oxide (CuO) nanostructures and control their morphology and size by rapid thermal decomposition of copper nitrate (CuN2O6) under ambient conditions. The size and morphology of the nanostructures can be controlled by changing the temperature and the duration of the decomposition process. The structure of the products was investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS). The results showed that the morphology of the nanostructures changed as the temperature was varied and their size increased with increasing the treatment time. The optical properties of the samples were investigated by UV-vis spectroscopy and a photoluminescence (PL) spectrometer. Rice-like nanostructures were observed and analyzed by X-ray photoelectron spectroscopy (XPS)/EDS and XRD which confirmed that the as-synthesized powders correspond to pure CuO.

AB - We report a novel method that allows the synthesis of copper oxide (CuO) nanostructures and control their morphology and size by rapid thermal decomposition of copper nitrate (CuN2O6) under ambient conditions. The size and morphology of the nanostructures can be controlled by changing the temperature and the duration of the decomposition process. The structure of the products was investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS). The results showed that the morphology of the nanostructures changed as the temperature was varied and their size increased with increasing the treatment time. The optical properties of the samples were investigated by UV-vis spectroscopy and a photoluminescence (PL) spectrometer. Rice-like nanostructures were observed and analyzed by X-ray photoelectron spectroscopy (XPS)/EDS and XRD which confirmed that the as-synthesized powders correspond to pure CuO.

KW - CuO

KW - Nanostructures

KW - Optical properties

KW - Thermal decomposition

UR - https://www.scopus.com/pages/publications/80051802836

U2 - 10.1016/j.jallcom.2011.06.056

DO - 10.1016/j.jallcom.2011.06.056

M3 - Article

AN - SCOPUS:80051802836

SN - 0925-8388

VL - 509

SP - 8761

EP - 8769

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 35

ER -

Synthesis and optical properties of CuO nanostructures obtained via a novel thermal decomposition method

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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