Synthesis and crystal structure of (Z)-ethyl 5-(phenylamino)-3- (phenylimino)-3H-1,2-dithiole-4-carboxylate

Mehtab Parveen; Sayed H. Mehdi; Mohammad N. Siddiqui; Mohammed B. Fettouhi

doi:10.1080/00397911.2010.518280

Synthesis and crystal structure of (Z)-ethyl 5-(phenylamino)-3- (phenylimino)-3H-1,2-dithiole-4-carboxylate

Mehtab Parveen^*
, Sayed H. Mehdi
, Mohammad N. Siddiqui
, Mohammed B. Fettouhi

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

The compound (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4- carboxylate 3 has been synthesized by the reaction of ethylacetoacetate 1 and phenylisothiocyanate 2. Its structure has been established by 1H NMR, 13C NMR, infrared, mass spectra, and X-ray crystallography.

Original language	English
Pages (from-to)	3469-3476
Number of pages	8
Journal	Synthetic Communications
Volume	41
Issue number	23
DOIs	https://doi.org/10.1080/00397911.2010.518280
State	Published - Jan 2011

Keywords

(Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1, 2-dithiole-4-carboxylate
Crystal structure
synthesis

ASJC Scopus subject areas

Organic Chemistry

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10.1080/00397911.2010.518280

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title = "Synthesis and crystal structure of (Z)-ethyl 5-(phenylamino)-3- (phenylimino)-3H-1,2-dithiole-4-carboxylate",

abstract = "The compound (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4- carboxylate 3 has been synthesized by the reaction of ethylacetoacetate 1 and phenylisothiocyanate 2. Its structure has been established by 1H NMR, 13C NMR, infrared, mass spectra, and X-ray crystallography.",

keywords = "(Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1, 2-dithiole-4-carboxylate, Crystal structure, synthesis",

author = "Mehtab Parveen and Mehdi, \{Sayed H.\} and Siddiqui, \{Mohammad N.\} and Fettouhi, \{Mohammed B.\}",

year = "2011",

month = jan,

doi = "10.1080/00397911.2010.518280",

language = "English",

volume = "41",

pages = "3469--3476",

journal = "Synthetic Communications",

issn = "0039-7911",

publisher = "Taylor and Francis Ltd.",

number = "23",

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TY - JOUR

T1 - Synthesis and crystal structure of (Z)-ethyl 5-(phenylamino)-3- (phenylimino)-3H-1,2-dithiole-4-carboxylate

AU - Parveen, Mehtab

AU - Mehdi, Sayed H.

AU - Siddiqui, Mohammad N.

AU - Fettouhi, Mohammed B.

PY - 2011/1

Y1 - 2011/1

N2 - The compound (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4- carboxylate 3 has been synthesized by the reaction of ethylacetoacetate 1 and phenylisothiocyanate 2. Its structure has been established by 1H NMR, 13C NMR, infrared, mass spectra, and X-ray crystallography.

AB - The compound (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4- carboxylate 3 has been synthesized by the reaction of ethylacetoacetate 1 and phenylisothiocyanate 2. Its structure has been established by 1H NMR, 13C NMR, infrared, mass spectra, and X-ray crystallography.

KW - (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1, 2-dithiole-4-carboxylate

KW - Crystal structure

KW - synthesis

UR - https://www.scopus.com/pages/publications/79961220429

U2 - 10.1080/00397911.2010.518280

DO - 10.1080/00397911.2010.518280

M3 - Article

AN - SCOPUS:79961220429

SN - 0039-7911

VL - 41

SP - 3469

EP - 3476

JO - Synthetic Communications

JF - Synthetic Communications

IS - 23

ER -

Synthesis and crystal structure of (Z)-ethyl 5-(phenylamino)-3- (phenylimino)-3H-1,2-dithiole-4-carboxylate

Abstract

Keywords

ASJC Scopus subject areas

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