Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles

Robin Chrystie; Felix Ebertz; Thomas Dreier; Christof Schulz

doi:10.1364/LACSEA.2018.LW3C.6

Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles

Robin Chrystie, Felix Ebertz, Thomas Dreier^*, Christof Schulz

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Silica nanoparticles are conveniently synthesized in gas phase H<inf>2</inf>/O<inf>2</inf> premixed flames and a silicon-carrying precursor (e.g., hexamethyldisiloxane, HMDSO). For flame kinetics mechanism validation including particle growth a technique for absolute concentration measurements of the intermediate SiO based on laser-induced fluorescence and Rayleigh scattering is demonstrated.

Original language	English
Title of host publication	Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018
Publisher	Optica Publishing Group (formerly OSA)
ISBN (Print)	9781943580446
DOIs	https://doi.org/10.1364/LACSEA.2018.LW3C.6
State	Published - 2018
Externally published	Yes

Publication series

Name	Optics InfoBase Conference Papers
Volume	Part F103-LACSEA 2018
ISSN (Electronic)	2162-2701

Bibliographical note

Publisher Copyright:
© 2018 The Author(s).

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Mechanics of Materials

Access to Document

10.1364/LACSEA.2018.LW3C.6

Cite this

Chrystie, R., Ebertz, F., Dreier, T., & Schulz, C. (2018). Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles. In Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018 (Optics InfoBase Conference Papers; Vol. Part F103-LACSEA 2018). Optica Publishing Group (formerly OSA). https://doi.org/10.1364/LACSEA.2018.LW3C.6

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title = "Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles",

abstract = "Silica nanoparticles are conveniently synthesized in gas phase H<inf>2</inf>/O<inf>2</inf> premixed flames and a silicon-carrying precursor (e.g., hexamethyldisiloxane, HMDSO). For flame kinetics mechanism validation including particle growth a technique for absolute concentration measurements of the intermediate SiO based on laser-induced fluorescence and Rayleigh scattering is demonstrated.",

author = "Robin Chrystie and Felix Ebertz and Thomas Dreier and Christof Schulz",

note = "Publisher Copyright: {\textcopyright} 2018 The Author(s).",

year = "2018",

doi = "10.1364/LACSEA.2018.LW3C.6",

language = "English",

isbn = "9781943580446",

series = "Optics InfoBase Conference Papers",

publisher = "Optica Publishing Group (formerly OSA)",

booktitle = "Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018",

}

Chrystie, R, Ebertz, F, Dreier, T & Schulz, C 2018, Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles. in Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018. Optics InfoBase Conference Papers, vol. Part F103-LACSEA 2018, Optica Publishing Group (formerly OSA). https://doi.org/10.1364/LACSEA.2018.LW3C.6

Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles. / Chrystie, Robin; Ebertz, Felix; Dreier, Thomas et al.
Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018. Optica Publishing Group (formerly OSA), 2018. (Optics InfoBase Conference Papers; Vol. Part F103-LACSEA 2018).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles

AU - Chrystie, Robin

AU - Ebertz, Felix

AU - Dreier, Thomas

AU - Schulz, Christof

PY - 2018

Y1 - 2018

N2 - Silica nanoparticles are conveniently synthesized in gas phase H<inf>2</inf>/O<inf>2</inf> premixed flames and a silicon-carrying precursor (e.g., hexamethyldisiloxane, HMDSO). For flame kinetics mechanism validation including particle growth a technique for absolute concentration measurements of the intermediate SiO based on laser-induced fluorescence and Rayleigh scattering is demonstrated.

AB - Silica nanoparticles are conveniently synthesized in gas phase H<inf>2</inf>/O<inf>2</inf> premixed flames and a silicon-carrying precursor (e.g., hexamethyldisiloxane, HMDSO). For flame kinetics mechanism validation including particle growth a technique for absolute concentration measurements of the intermediate SiO based on laser-induced fluorescence and Rayleigh scattering is demonstrated.

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U2 - 10.1364/LACSEA.2018.LW3C.6

DO - 10.1364/LACSEA.2018.LW3C.6

M3 - Conference contribution

AN - SCOPUS:85051255444

SN - 9781943580446

T3 - Optics InfoBase Conference Papers

BT - Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018

PB - Optica Publishing Group (formerly OSA)

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Chrystie R, Ebertz F, Dreier T, Schulz C. Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles. In Laser Applications to Chemical, Security and Environmental Analysis, LACSEA 2018. Optica Publishing Group (formerly OSA). 2018. (Optics InfoBase Conference Papers). doi: 10.1364/LACSEA.2018.LW3C.6

Strategy for determining absolute concentration levels of SiO in low pressure gas phase synthesis flames for silica nanoparticles

Abstract

Publication series

Bibliographical note

ASJC Scopus subject areas

Access to Document

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Cite this