Solid-state NMR studies of 1,3-imidazolidine-2-selenone and some related compounds

Mohamed I.M. Wazeer; Anvarhusein A. Isab; Herman P. Perzanowski

doi:10.1002/mrc.1305

Solid-state NMR studies of 1,3-imidazolidine-2-selenone and some related compounds

Mohamed I.M. Wazeer^*, Anvarhusein A. Isab, Herman P. Perzanowski

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

Solid-state cross-polarization magic angle spinning ¹³C, ⁷⁷Se and ¹⁵N NMR spectra were recorded for 1,3-imidazolidine-2-selenone, its N-substituted derivatives and some related compounds. The spinning sideband manifold intensities were used to obtain principal values of ¹³C and ⁷⁷Se chemical shift tensors. Large selenium chemical shift anisotropies were observed for these selenones.

Original language	English
Pages (from-to)	1026-1029
Number of pages	4
Journal	Magnetic Resonance in Chemistry
Volume	41
Issue number	12
DOIs	https://doi.org/10.1002/mrc.1305
State	Published - Dec 2003

Keywords

1,3-diazepine-2-selenone
1,3-diazinane-2-selenone
1,3-imidazolidine-2-selenone
C NMR
Chemical shift anisotropy
Cross-polarization magic angle spinning
N NMR
Se NMR
Solid-state NMR

ASJC Scopus subject areas

General Chemistry
General Materials Science

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10.1002/mrc.1305

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@article{c1a2450c0cec4da6906d90399bf2fab0,

title = "Solid-state NMR studies of 1,3-imidazolidine-2-selenone and some related compounds",

abstract = "Solid-state cross-polarization magic angle spinning 13C, 77Se and 15N NMR spectra were recorded for 1,3-imidazolidine-2-selenone, its N-substituted derivatives and some related compounds. The spinning sideband manifold intensities were used to obtain principal values of 13C and 77Se chemical shift tensors. Large selenium chemical shift anisotropies were observed for these selenones.",

keywords = "1,3-diazepine-2-selenone, 1,3-diazinane-2-selenone, 1,3-imidazolidine-2-selenone, C NMR, Chemical shift anisotropy, Cross-polarization magic angle spinning, N NMR, Se NMR, Solid-state NMR",

author = "Wazeer, {Mohamed I.M.} and Isab, {Anvarhusein A.} and Perzanowski, {Herman P.}",

year = "2003",

month = dec,

doi = "10.1002/mrc.1305",

language = "English",

volume = "41",

pages = "1026--1029",

journal = "Magnetic Resonance in Chemistry",

issn = "0749-1581",

publisher = "John Wiley and Sons Ltd",

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T1 - Solid-state NMR studies of 1,3-imidazolidine-2-selenone and some related compounds

AU - Wazeer, Mohamed I.M.

AU - Isab, Anvarhusein A.

AU - Perzanowski, Herman P.

PY - 2003/12

Y1 - 2003/12

N2 - Solid-state cross-polarization magic angle spinning 13C, 77Se and 15N NMR spectra were recorded for 1,3-imidazolidine-2-selenone, its N-substituted derivatives and some related compounds. The spinning sideband manifold intensities were used to obtain principal values of 13C and 77Se chemical shift tensors. Large selenium chemical shift anisotropies were observed for these selenones.

AB - Solid-state cross-polarization magic angle spinning 13C, 77Se and 15N NMR spectra were recorded for 1,3-imidazolidine-2-selenone, its N-substituted derivatives and some related compounds. The spinning sideband manifold intensities were used to obtain principal values of 13C and 77Se chemical shift tensors. Large selenium chemical shift anisotropies were observed for these selenones.

KW - 1,3-diazepine-2-selenone

KW - 1,3-diazinane-2-selenone

KW - 1,3-imidazolidine-2-selenone

KW - C NMR

KW - Chemical shift anisotropy

KW - Cross-polarization magic angle spinning

KW - N NMR

KW - Se NMR

KW - Solid-state NMR

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U2 - 10.1002/mrc.1305

DO - 10.1002/mrc.1305

M3 - Article

AN - SCOPUS:0347384218

SN - 0749-1581

VL - 41

SP - 1026

EP - 1029

JO - Magnetic Resonance in Chemistry

JF - Magnetic Resonance in Chemistry

IS - 12

ER -

Solid-state NMR studies of 1,3-imidazolidine-2-selenone and some related compounds

Abstract

Keywords

ASJC Scopus subject areas

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