Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine

Esra Durduran; Huseyin Altundag; Mustafa Imamoglu; Salih Zeki Yildiz; Mustafa Tuzen

doi:10.1016/j.jiec.2014.12.041

Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine

Esra Durduran
, Huseyin Altundag^*
, Mustafa Imamoglu
, Salih Zeki Yildiz
, Mustafa Tuzen

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

52 Scopus citations

Abstract

Silica gel was functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine group (AEDHB-SG) and characterized by elemental analysis and FT-IR spectroscopy. Preconcentration conditions of Cd(II), Cu(II), Ni(II) and Pb(II) were investigated on the AEDHB-SG loaded column using a solid phase extraction technique. The effects of parameters such as the pH, sample volume, flow rates, matrix ions were examined. Adsorption capacity of AEDHB-SG for Cd(II), Cu(II), Ni(II) and Pb(II) was 0.40, 0.56, 0.50 and 0.23mmolg^-1. The accuracy of the developed method was confirmed by certified reference materials. Optimized method was applied to water and food samples for the determination of trace metals using ICP-OES.

Original language	English
Pages (from-to)	245-250
Number of pages	6
Journal	Journal of Industrial and Engineering Chemistry
Volume	27
DOIs	https://doi.org/10.1016/j.jiec.2014.12.041
State	Published - 25 Jul 2015
Externally published	Yes

Bibliographical note

Publisher Copyright:
© 2015 The Korean Society of Industrial and Engineering Chemistry.

Keywords

ICP-OES
Modified silica gel
Preconcentration
Trace metals
Water and food samples

ASJC Scopus subject areas

General Chemical Engineering

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10.1016/j.jiec.2014.12.041

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@article{1a1cfc37e5cb45b580bd6ec8a3de356f,

title = "Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine",

abstract = "Silica gel was functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine group (AEDHB-SG) and characterized by elemental analysis and FT-IR spectroscopy. Preconcentration conditions of Cd(II), Cu(II), Ni(II) and Pb(II) were investigated on the AEDHB-SG loaded column using a solid phase extraction technique. The effects of parameters such as the pH, sample volume, flow rates, matrix ions were examined. Adsorption capacity of AEDHB-SG for Cd(II), Cu(II), Ni(II) and Pb(II) was 0.40, 0.56, 0.50 and 0.23mmolg-1. The accuracy of the developed method was confirmed by certified reference materials. Optimized method was applied to water and food samples for the determination of trace metals using ICP-OES.",

keywords = "ICP-OES, Modified silica gel, Preconcentration, Trace metals, Water and food samples",

author = "Esra Durduran and Huseyin Altundag and Mustafa Imamoglu and Yildiz, \{Salih Zeki\} and Mustafa Tuzen",

note = "Publisher Copyright: {\textcopyright} 2015 The Korean Society of Industrial and Engineering Chemistry.",

year = "2015",

month = jul,

day = "25",

doi = "10.1016/j.jiec.2014.12.041",

language = "English",

volume = "27",

pages = "245--250",

journal = "Journal of Industrial and Engineering Chemistry",

issn = "1226-086X",

publisher = "Korean Society of Industrial Engineering Chemistry",

}

Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine. / Durduran, Esra; Altundag, Huseyin; Imamoglu, Mustafa et al.
In: Journal of Industrial and Engineering Chemistry, Vol. 27, 25.07.2015, p. 245-250.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine

AU - Durduran, Esra

AU - Altundag, Huseyin

AU - Imamoglu, Mustafa

AU - Yildiz, Salih Zeki

AU - Tuzen, Mustafa

PY - 2015/7/25

Y1 - 2015/7/25

N2 - Silica gel was functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine group (AEDHB-SG) and characterized by elemental analysis and FT-IR spectroscopy. Preconcentration conditions of Cd(II), Cu(II), Ni(II) and Pb(II) were investigated on the AEDHB-SG loaded column using a solid phase extraction technique. The effects of parameters such as the pH, sample volume, flow rates, matrix ions were examined. Adsorption capacity of AEDHB-SG for Cd(II), Cu(II), Ni(II) and Pb(II) was 0.40, 0.56, 0.50 and 0.23mmolg-1. The accuracy of the developed method was confirmed by certified reference materials. Optimized method was applied to water and food samples for the determination of trace metals using ICP-OES.

AB - Silica gel was functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine group (AEDHB-SG) and characterized by elemental analysis and FT-IR spectroscopy. Preconcentration conditions of Cd(II), Cu(II), Ni(II) and Pb(II) were investigated on the AEDHB-SG loaded column using a solid phase extraction technique. The effects of parameters such as the pH, sample volume, flow rates, matrix ions were examined. Adsorption capacity of AEDHB-SG for Cd(II), Cu(II), Ni(II) and Pb(II) was 0.40, 0.56, 0.50 and 0.23mmolg-1. The accuracy of the developed method was confirmed by certified reference materials. Optimized method was applied to water and food samples for the determination of trace metals using ICP-OES.

KW - ICP-OES

KW - Modified silica gel

KW - Preconcentration

KW - Trace metals

KW - Water and food samples

UR - https://www.scopus.com/pages/publications/84930794015

U2 - 10.1016/j.jiec.2014.12.041

DO - 10.1016/j.jiec.2014.12.041

M3 - Article

AN - SCOPUS:84930794015

SN - 1226-086X

VL - 27

SP - 245

EP - 250

JO - Journal of Industrial and Engineering Chemistry

JF - Journal of Industrial and Engineering Chemistry

ER -

Simultaneous ICP-OES determination of trace metals in water and food samples after their preconcentration on silica gel functionalized with N-(2-aminoethyl)-2,3-dihydroxybenzaldimine

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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