Material characterization and bioactivity evaluation of dental porcelain modified by bioactive glass

Marianthi Manda; Ourania Menti Goudouri; Lambrini Papadopoulou; Nikolaos Kantiranis; Dimitris Christofilos; Konstantinos Triantafyllidis; Konstantinos M. Paraskevopoulos; Petros Koidis

doi:10.1016/j.ceramint.2012.03.078

Material characterization and bioactivity evaluation of dental porcelain modified by bioactive glass

Marianthi Manda
, Ourania Menti Goudouri
, Lambrini Papadopoulou
, Nikolaos Kantiranis
, Dimitris Christofilos
, Konstantinos Triantafyllidis
, Konstantinos M. Paraskevopoulos
, Petros Koidis^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

14 Scopus citations

Abstract

This study aimed at the chemical, microstructural and textural characterization of the sol-gel derived dental porcelain modified by bioactive glass and the evaluation of its bioactivity. Sol-gel derived specimens of the composite material were constructed and subjected to firing cycle. Specimens of bioactive glass and dental porcelain served as control. All the specimens were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS) and N ₂ porosimetry. The assessment of in vitro bioactivity was carried out by incubating the composite specimens in DMEM solution. Apatite formation was evaluated by SEM/EDS, FTIR and XRD analysis. Microstructural analysis by SEM revealed irregularly shaped particles with broad size distribution, while complex porei network with large pore volume and non-uniform pore size distribution was evident. N ₂-adsorption isotherms were representative of non-nano-/meso-porous materials. A mixture of a- and b-wollastonite, apatite and leucite phases were detected by FTIR and Raman spectroscopy. The XRD analysis confirmed the previous results, though traces of cristobalite were identified too. The in vitro tests evidenced the bioactivity of the specimens in a 3-day-period. In conclusion, the physicochemical properties of the sol-gel derived composite result in a bioactive material, though further modifications need to be considered in order to fulfill the requirements of application in the clinical reality.

Original language	English
Pages (from-to)	5585-5596
Number of pages	12
Journal	Ceramics International
Volume	38
Issue number	7
DOIs	https://doi.org/10.1016/j.ceramint.2012.03.078
State	Published - Sep 2012
Externally published	Yes

Keywords

A. Sol-gel process
D. Apatite
D. Porcelain
E. Biomedical applications

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

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10.1016/j.ceramint.2012.03.078

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title = "Material characterization and bioactivity evaluation of dental porcelain modified by bioactive glass",

abstract = "This study aimed at the chemical, microstructural and textural characterization of the sol-gel derived dental porcelain modified by bioactive glass and the evaluation of its bioactivity. Sol-gel derived specimens of the composite material were constructed and subjected to firing cycle. Specimens of bioactive glass and dental porcelain served as control. All the specimens were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS) and N 2 porosimetry. The assessment of in vitro bioactivity was carried out by incubating the composite specimens in DMEM solution. Apatite formation was evaluated by SEM/EDS, FTIR and XRD analysis. Microstructural analysis by SEM revealed irregularly shaped particles with broad size distribution, while complex porei network with large pore volume and non-uniform pore size distribution was evident. N 2-adsorption isotherms were representative of non-nano-/meso-porous materials. A mixture of a- and b-wollastonite, apatite and leucite phases were detected by FTIR and Raman spectroscopy. The XRD analysis confirmed the previous results, though traces of cristobalite were identified too. The in vitro tests evidenced the bioactivity of the specimens in a 3-day-period. In conclusion, the physicochemical properties of the sol-gel derived composite result in a bioactive material, though further modifications need to be considered in order to fulfill the requirements of application in the clinical reality.",

keywords = "A. Sol-gel process, D. Apatite, D. Porcelain, E. Biomedical applications",

author = "Marianthi Manda and Goudouri, \{Ourania Menti\} and Lambrini Papadopoulou and Nikolaos Kantiranis and Dimitris Christofilos and Konstantinos Triantafyllidis and Paraskevopoulos, \{Konstantinos M.\} and Petros Koidis",

year = "2012",

month = sep,

doi = "10.1016/j.ceramint.2012.03.078",

language = "English",

volume = "38",

pages = "5585--5596",

journal = "Ceramics International",

issn = "0272-8842",

publisher = "Elsevier Ltd.",

number = "7",

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TY - JOUR

T1 - Material characterization and bioactivity evaluation of dental porcelain modified by bioactive glass

AU - Manda, Marianthi

AU - Goudouri, Ourania Menti

AU - Papadopoulou, Lambrini

AU - Kantiranis, Nikolaos

AU - Christofilos, Dimitris

AU - Triantafyllidis, Konstantinos

AU - Paraskevopoulos, Konstantinos M.

AU - Koidis, Petros

PY - 2012/9

Y1 - 2012/9

N2 - This study aimed at the chemical, microstructural and textural characterization of the sol-gel derived dental porcelain modified by bioactive glass and the evaluation of its bioactivity. Sol-gel derived specimens of the composite material were constructed and subjected to firing cycle. Specimens of bioactive glass and dental porcelain served as control. All the specimens were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS) and N 2 porosimetry. The assessment of in vitro bioactivity was carried out by incubating the composite specimens in DMEM solution. Apatite formation was evaluated by SEM/EDS, FTIR and XRD analysis. Microstructural analysis by SEM revealed irregularly shaped particles with broad size distribution, while complex porei network with large pore volume and non-uniform pore size distribution was evident. N 2-adsorption isotherms were representative of non-nano-/meso-porous materials. A mixture of a- and b-wollastonite, apatite and leucite phases were detected by FTIR and Raman spectroscopy. The XRD analysis confirmed the previous results, though traces of cristobalite were identified too. The in vitro tests evidenced the bioactivity of the specimens in a 3-day-period. In conclusion, the physicochemical properties of the sol-gel derived composite result in a bioactive material, though further modifications need to be considered in order to fulfill the requirements of application in the clinical reality.

AB - This study aimed at the chemical, microstructural and textural characterization of the sol-gel derived dental porcelain modified by bioactive glass and the evaluation of its bioactivity. Sol-gel derived specimens of the composite material were constructed and subjected to firing cycle. Specimens of bioactive glass and dental porcelain served as control. All the specimens were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS) and N 2 porosimetry. The assessment of in vitro bioactivity was carried out by incubating the composite specimens in DMEM solution. Apatite formation was evaluated by SEM/EDS, FTIR and XRD analysis. Microstructural analysis by SEM revealed irregularly shaped particles with broad size distribution, while complex porei network with large pore volume and non-uniform pore size distribution was evident. N 2-adsorption isotherms were representative of non-nano-/meso-porous materials. A mixture of a- and b-wollastonite, apatite and leucite phases were detected by FTIR and Raman spectroscopy. The XRD analysis confirmed the previous results, though traces of cristobalite were identified too. The in vitro tests evidenced the bioactivity of the specimens in a 3-day-period. In conclusion, the physicochemical properties of the sol-gel derived composite result in a bioactive material, though further modifications need to be considered in order to fulfill the requirements of application in the clinical reality.

KW - A. Sol-gel process

KW - D. Apatite

KW - D. Porcelain

KW - E. Biomedical applications

UR - https://www.scopus.com/pages/publications/84862694166

U2 - 10.1016/j.ceramint.2012.03.078

DO - 10.1016/j.ceramint.2012.03.078

M3 - Article

AN - SCOPUS:84862694166

SN - 0272-8842

VL - 38

SP - 5585

EP - 5596

JO - Ceramics International

JF - Ceramics International

IS - 7

ER -

Material characterization and bioactivity evaluation of dental porcelain modified by bioactive glass

Abstract

Keywords

ASJC Scopus subject areas

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