Abstract
In the present study, spectrophotometric determination of uranyl with 2-(5-Bromo-2-pyridylazo)-5-(diethylamino) phenol after ionic liquid based microextraction has been developed. Effect of experimental parameters were optimized to achieve high sensitivity and stability of the complex. The analytical parameters such as linear range (1.33–670 µg L−1), limit of detection (0.97 µg L−1) and enrichment factor (150) were calculated for the method. The relative standard deviation of ten replicate measurement of uranyl was 6.53 and 2.59 % for 66 and 133 µg L−1 uranium, respectively. The proposed method was used to determine the uranyl ions in spiked water samples.
Original language | English |
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Pages (from-to) | 385-392 |
Number of pages | 8 |
Journal | Journal of Radioanalytical and Nuclear Chemistry |
Volume | 306 |
Issue number | 2 |
DOIs | |
State | Published - 1 Nov 2015 |
Externally published | Yes |
Bibliographical note
Publisher Copyright:© 2015, Akadémiai Kiadó, Budapest, Hungary.
Keywords
- Br PADAP
- Ionic liquid
- Microextraction
- Spectrophotometer
- Uranyl
ASJC Scopus subject areas
- Analytical Chemistry
- Nuclear Energy and Engineering
- Radiology Nuclear Medicine and imaging
- Pollution
- Spectroscopy
- Public Health, Environmental and Occupational Health
- Health, Toxicology and Mutagenesis