Functionalization of tungsten oxide into MWCNT and its application for sunlight-induced degradation of rhodamine B

Tawfik A. Saleh, Vinod K. Gupta*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

556 Scopus citations

Abstract

A composite of multi-walled carbon nanotube/tungsten oxide (MWCNT/WO 3) has been successfully synthesized. The prepared composite was characterized by X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), high-resolution transmission electron microscopy (HRTEM) and Fourier transform infrared spectroscopy (FTIR). The catalytic activity was investigated by rhodamine B degradation under solar irradiation. The influence of various degradation parameters such as solar illumination time, initial dye concentration, dosage and pH was investigated. It was found that the composite exhibits an enhanced photocatalytic activity as compared with WO 3 and a mechanical mixture of MWCNTs and WO 3. The enhancement in photocatalytic performance of the MWCNT/WO 3 composite has been explained based on adsorption ability and electron transportation as a result of a strong interaction between WO 3 and MWCNTs. Besides, MWCNTs acts as dispersing agent preventing WO 3 from agglomerating during the catalytic process, providing a high active surface area of the catalyst. A reasonable mechanism for the enhanced reactivity was proposed.

Original languageEnglish
Pages (from-to)337-344
Number of pages8
JournalJournal of Colloid and Interface Science
Volume362
Issue number2
DOIs
StatePublished - 15 Oct 2011

Bibliographical note

Funding Information:
Tawfik A. Saleh acknowledges the support of King Fahd University of Petroleum and Minerals, (KFUPM) Dhahran, Saudi Arabia for this work.

Keywords

  • Degradation
  • Multi-walled carbon nanotube
  • Rhodamine B
  • Tungsten oxide

ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials
  • Biomaterials
  • Surfaces, Coatings and Films
  • Colloid and Surface Chemistry

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