Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples

Ruspika Sundaresan; Vinitha Mariyappan; Shen Ming Chen; Saranvignesh Alagarsamy; Muthumariappan Akilarasan

doi:10.3390/mi13060876

Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples

Ruspika Sundaresan
, Vinitha Mariyappan
, Shen Ming Chen^*
, Saranvignesh Alagarsamy
, Muthumariappan Akilarasan

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

8 Scopus citations

Abstract

This study utilized a simple hydrothermal method to synthesize nickel molybdenum oxide (NMO) for the detection of furazolidone (FZE). Our synthesized NMO was characterized by X-Ray diffraction (XRD), X-Ray photoelectron spectroscopy (XPS), Raman spectroscopy, Fourier trans-form infrared spectroscopy (FTIR), field emission scanning electron spectroscopy (FE-SEM), and energy dispersive X-Ray spectroscopy (EDX). The cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used to detect the FZE. Under optimized conditions, the obtained results showed that the NMO had an excellent electrocatalytic property towards FZE. As a result, NMO/GCE showed a good linear range of 0.001–1765 µM, an excellent detection limit (LOD) of 0.02 µM, and sensitivity of 0.2042 µA µM⁻¹ cm⁻².

Original language	English
Article number	876
Journal	Micromachines
Volume	13
Issue number	6
DOIs	https://doi.org/10.3390/mi13060876
State	Published - Jun 2022
Externally published	Yes

Bibliographical note

Publisher Copyright:
© 2022 by the authors. Licensee MDPI, Basel, Switzerland.

Keywords

bimetal oxide
cyclic voltammetry
furazolidone
glassy carbon electrode
hydrothermal

ASJC Scopus subject areas

Control and Systems Engineering
Mechanical Engineering
Electrical and Electronic Engineering

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10.3390/mi13060876

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@article{0d6260e382324ed295dc57eda93fd586,

title = "Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples",

abstract = "This study utilized a simple hydrothermal method to synthesize nickel molybdenum oxide (NMO) for the detection of furazolidone (FZE). Our synthesized NMO was characterized by X-Ray diffraction (XRD), X-Ray photoelectron spectroscopy (XPS), Raman spectroscopy, Fourier trans-form infrared spectroscopy (FTIR), field emission scanning electron spectroscopy (FE-SEM), and energy dispersive X-Ray spectroscopy (EDX). The cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used to detect the FZE. Under optimized conditions, the obtained results showed that the NMO had an excellent electrocatalytic property towards FZE. As a result, NMO/GCE showed a good linear range of 0.001–1765 µM, an excellent detection limit (LOD) of 0.02 µM, and sensitivity of 0.2042 µA µM−1 cm−2.",

keywords = "bimetal oxide, cyclic voltammetry, furazolidone, glassy carbon electrode, hydrothermal",

author = "Ruspika Sundaresan and Vinitha Mariyappan and Chen, \{Shen Ming\} and Saranvignesh Alagarsamy and Muthumariappan Akilarasan",

note = "Publisher Copyright: {\textcopyright} 2022 by the authors. Licensee MDPI, Basel, Switzerland.",

year = "2022",

month = jun,

doi = "10.3390/mi13060876",

language = "English",

volume = "13",

journal = "Micromachines",

issn = "2072-666X",

publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",

number = "6",

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TY - JOUR

T1 - Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples

AU - Sundaresan, Ruspika

AU - Mariyappan, Vinitha

AU - Chen, Shen Ming

AU - Alagarsamy, Saranvignesh

AU - Akilarasan, Muthumariappan

PY - 2022/6

Y1 - 2022/6

N2 - This study utilized a simple hydrothermal method to synthesize nickel molybdenum oxide (NMO) for the detection of furazolidone (FZE). Our synthesized NMO was characterized by X-Ray diffraction (XRD), X-Ray photoelectron spectroscopy (XPS), Raman spectroscopy, Fourier trans-form infrared spectroscopy (FTIR), field emission scanning electron spectroscopy (FE-SEM), and energy dispersive X-Ray spectroscopy (EDX). The cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used to detect the FZE. Under optimized conditions, the obtained results showed that the NMO had an excellent electrocatalytic property towards FZE. As a result, NMO/GCE showed a good linear range of 0.001–1765 µM, an excellent detection limit (LOD) of 0.02 µM, and sensitivity of 0.2042 µA µM−1 cm−2.

AB - This study utilized a simple hydrothermal method to synthesize nickel molybdenum oxide (NMO) for the detection of furazolidone (FZE). Our synthesized NMO was characterized by X-Ray diffraction (XRD), X-Ray photoelectron spectroscopy (XPS), Raman spectroscopy, Fourier trans-form infrared spectroscopy (FTIR), field emission scanning electron spectroscopy (FE-SEM), and energy dispersive X-Ray spectroscopy (EDX). The cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used to detect the FZE. Under optimized conditions, the obtained results showed that the NMO had an excellent electrocatalytic property towards FZE. As a result, NMO/GCE showed a good linear range of 0.001–1765 µM, an excellent detection limit (LOD) of 0.02 µM, and sensitivity of 0.2042 µA µM−1 cm−2.

KW - bimetal oxide

KW - cyclic voltammetry

KW - furazolidone

KW - glassy carbon electrode

KW - hydrothermal

UR - https://www.scopus.com/pages/publications/85131809885

U2 - 10.3390/mi13060876

DO - 10.3390/mi13060876

M3 - Article

AN - SCOPUS:85131809885

SN - 2072-666X

VL - 13

JO - Micromachines

JF - Micromachines

IS - 6

M1 - 876

ER -

Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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