Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane

Mohammed B. Alshammari; Ashraf A. Aly; Stefan Bräse; Martin Nieger; Lamiaa E. Abd El-Haleem

doi:10.1021/acsomega.2c00141

Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane

Mohammed B. Alshammari
, Ashraf A. Aly
, Stefan Bräse
, Martin Nieger
, Lamiaa E. Abd El-Haleem

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.

Original language	English
Pages (from-to)	12879-12890
Number of pages	12
Journal	ACS Omega
Volume	7
Issue number	15
DOIs	https://doi.org/10.1021/acsomega.2c00141
State	Published - 19 Apr 2022
Externally published	Yes

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© 2022 American Chemical Society. All rights reserved.

ASJC Scopus subject areas

General Chemistry
General Chemical Engineering

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title = "Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane",

abstract = "The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.",

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doi = "10.1021/acsomega.2c00141",

language = "English",

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T1 - Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane

AU - Alshammari, Mohammed B.

AU - Aly, Ashraf A.

AU - Bräse, Stefan

AU - Nieger, Martin

AU - Abd El-Haleem, Lamiaa E.

PY - 2022/4/19

Y1 - 2022/4/19

N2 - The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.

AB - The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.

UR - https://www.scopus.com/pages/publications/85128535653

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DO - 10.1021/acsomega.2c00141

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JO - ACS Omega

JF - ACS Omega

IS - 15

ER -

Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane

Abstract

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ASJC Scopus subject areas

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