Dispersive liquid–liquid microextraction–spectrophotometry combination for determination of rhodamine B in food, water, and environmental samples

Yunus Emre Unsal; Mustafa Soylak; Mustafa Tuzen

doi:10.1080/19443994.2014.930699

Dispersive liquid–liquid microextraction–spectrophotometry combination for determination of rhodamine B in food, water, and environmental samples

Yunus Emre Unsal, Mustafa Soylak^*, Mustafa Tuzen

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

30 Scopus citations

Abstract

Abstract: A new dispersive liquid–liquid microextraction procedure combined with UV–visible spectrophotometry is described for sensitive and selective determination of rhodamine B. Various analytical parameters such as pH, extraction and dispersive solvents type and volume, sample volumes, and extraction time were optimized. Matrix effects of concomitants were also examined. Preconcentration factor was found to be 330. Detection limit was calculated as 2.1 μg L⁻¹. The relative standard deviation was found to be 4%. The validation of the developed procedure was checked by the addition/recovery tests. The procedure was successfully performed to the determination of trace levels of rhodamine B in drug, ink, food, cosmetic product, and waste waters.

Original language	English
Pages (from-to)	2103-2108
Number of pages	6
Journal	Desalination and Water Treatment
Volume	55
Issue number	8
DOIs	https://doi.org/10.1080/19443994.2014.930699
State	Published - 21 Aug 2015
Externally published	Yes

Bibliographical note

Publisher Copyright:
© 2014 Balaban Desalination Publications. All rights reserved.

Keywords

Cosmetic
Drug
Food
Microextraction
Rhodamine B
Spectrophotometry
Waste water

ASJC Scopus subject areas

Water Science and Technology
Ocean Engineering
Pollution

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

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10.1080/19443994.2014.930699

Cite this

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title = "Dispersive liquid–liquid microextraction–spectrophotometry combination for determination of rhodamine B in food, water, and environmental samples",

abstract = "Abstract: A new dispersive liquid–liquid microextraction procedure combined with UV–visible spectrophotometry is described for sensitive and selective determination of rhodamine B. Various analytical parameters such as pH, extraction and dispersive solvents type and volume, sample volumes, and extraction time were optimized. Matrix effects of concomitants were also examined. Preconcentration factor was found to be 330. Detection limit was calculated as 2.1 μg L−1. The relative standard deviation was found to be 4\%. The validation of the developed procedure was checked by the addition/recovery tests. The procedure was successfully performed to the determination of trace levels of rhodamine B in drug, ink, food, cosmetic product, and waste waters.",

keywords = "Cosmetic, Drug, Food, Microextraction, Rhodamine B, Spectrophotometry, Waste water",

author = "Unsal, \{Yunus Emre\} and Mustafa Soylak and Mustafa Tuzen",

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doi = "10.1080/19443994.2014.930699",

language = "English",

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journal = "Desalination and Water Treatment",

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TY - JOUR

T1 - Dispersive liquid–liquid microextraction–spectrophotometry combination for determination of rhodamine B in food, water, and environmental samples

AU - Unsal, Yunus Emre

AU - Soylak, Mustafa

AU - Tuzen, Mustafa

PY - 2015/8/21

Y1 - 2015/8/21

N2 - Abstract: A new dispersive liquid–liquid microextraction procedure combined with UV–visible spectrophotometry is described for sensitive and selective determination of rhodamine B. Various analytical parameters such as pH, extraction and dispersive solvents type and volume, sample volumes, and extraction time were optimized. Matrix effects of concomitants were also examined. Preconcentration factor was found to be 330. Detection limit was calculated as 2.1 μg L−1. The relative standard deviation was found to be 4%. The validation of the developed procedure was checked by the addition/recovery tests. The procedure was successfully performed to the determination of trace levels of rhodamine B in drug, ink, food, cosmetic product, and waste waters.

AB - Abstract: A new dispersive liquid–liquid microextraction procedure combined with UV–visible spectrophotometry is described for sensitive and selective determination of rhodamine B. Various analytical parameters such as pH, extraction and dispersive solvents type and volume, sample volumes, and extraction time were optimized. Matrix effects of concomitants were also examined. Preconcentration factor was found to be 330. Detection limit was calculated as 2.1 μg L−1. The relative standard deviation was found to be 4%. The validation of the developed procedure was checked by the addition/recovery tests. The procedure was successfully performed to the determination of trace levels of rhodamine B in drug, ink, food, cosmetic product, and waste waters.

KW - Cosmetic

KW - Drug

KW - Food

KW - Microextraction

KW - Rhodamine B

KW - Spectrophotometry

KW - Waste water

UR - https://www.scopus.com/pages/publications/84939651055

U2 - 10.1080/19443994.2014.930699

DO - 10.1080/19443994.2014.930699

M3 - Article

AN - SCOPUS:84939651055

SN - 1944-3994

VL - 55

SP - 2103

EP - 2108

JO - Desalination and Water Treatment

JF - Desalination and Water Treatment

IS - 8

ER -

Dispersive liquid–liquid microextraction–spectrophotometry combination for determination of rhodamine B in food, water, and environmental samples

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

UN SDGs

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