Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis

M. S.H. Choudhury; Mohammad Shahidul Alam; Md Mizanul Islam; Tetsuo Soga; M. Shafiul Alam; Mohammad Rafiqul Islam

doi:10.1109/ICISET.2018.8745655

Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis

M. S.H. Choudhury, Mohammad Shahidul Alam, Md Mizanul Islam, Tetsuo Soga, M. Shafiul Alam, Mohammad Rafiqul Islam

Applied Research Center for Environment and Marine Studies

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

3 Scopus citations

Abstract

In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ϵ) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.

Original language	English
Title of host publication	2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018
Publisher	Institute of Electrical and Electronics Engineers Inc.
Pages	257-261
Number of pages	5
ISBN (Electronic)	9781538685242
DOIs	https://doi.org/10.1109/ICISET.2018.8745655
State	Published - Oct 2018

Publication series

Name	2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018

Bibliographical note

Publisher Copyright:
© 2018 IEEE.

Keywords

SSP method
W-H analysis
X-ray diffraction (XRD)
ZnO nanoparticles

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Instrumentation
Computer Networks and Communications
Computer Science Applications
Energy Engineering and Power Technology
Electrical and Electronic Engineering

Access to Document

10.1109/ICISET.2018.8745655

Cite this

Choudhury, M. S. H., Alam, M. S., Mizanul Islam, M., Soga, T., Shafiul Alam, M., & Islam, M. R. (2018). Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis. In 2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018 (pp. 257-261). Article 8745655 (2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018). Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/ICISET.2018.8745655

Choudhury, M. S.H. ; Alam, Mohammad Shahidul ; Mizanul Islam, Md et al. / Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis. 2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018. Institute of Electrical and Electronics Engineers Inc., 2018. pp. 257-261 (2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018).

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title = "Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis",

abstract = "In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ϵ) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.",

keywords = "SSP method, W-H analysis, X-ray diffraction (XRD), ZnO nanoparticles",

author = "Choudhury, \{M. S.H.\} and Alam, \{Mohammad Shahidul\} and \{Mizanul Islam\}, Md and Tetsuo Soga and \{Shafiul Alam\}, M. and Islam, \{Mohammad Rafiqul\}",

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year = "2018",

month = oct,

doi = "10.1109/ICISET.2018.8745655",

language = "English",

series = "2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018",

publisher = "Institute of Electrical and Electronics Engineers Inc.",

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Choudhury, MSH, Alam, MS, Mizanul Islam, M, Soga, T, Shafiul Alam, M & Islam, MR 2018, Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis. in 2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018., 8745655, 2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018, Institute of Electrical and Electronics Engineers Inc., pp. 257-261. https://doi.org/10.1109/ICISET.2018.8745655

Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis. / Choudhury, M. S.H.; Alam, Mohammad Shahidul; Mizanul Islam, Md et al.
2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018. Institute of Electrical and Electronics Engineers Inc., 2018. p. 257-261 8745655 (2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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T1 - Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis

AU - Choudhury, M. S.H.

AU - Alam, Mohammad Shahidul

AU - Mizanul Islam, Md

AU - Soga, Tetsuo

AU - Shafiul Alam, M.

AU - Islam, Mohammad Rafiqul

PY - 2018/10

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N2 - In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ϵ) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.

AB - In this study, the blade coating technique was used for gettinge ZnO films and characterized using X-ray diffraction (XRD) analysis. The analysis indicated that ZnO particle was crystallite nature along with a usual hexagonal wurtzite sturcture. The X-ray peak profile analysis (XPPA) was used to validate the crystallite development. Williamson-Hall (W-H) and size-strain plot (SSP) analysis were implemented to determine the crystallite sizes (D) and the lattice strain (ϵ) of ZnO nanoparticles. XRD peaks were further studied to determine the some of the physical parameters including lattice strain, crystal stress, and energy density. Here, we have calculated the above mentioned parameters using few modified forms of W-H models and compared the results of the parameters that have been obtained from various methods. The study reveals that the crystallite parameters evaluated from various model are almost similar.

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Choudhury MSH, Alam MS, Mizanul Islam M, Soga T, Shafiul Alam M, Islam MR. Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis. In 2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018. Institute of Electrical and Electronics Engineers Inc. 2018. p. 257-261. 8745655. (2018 International Conference on Innovations in Science, Engineering and Technology, ICISET 2018). doi: 10.1109/ICISET.2018.8745655

Determining Crystallite Parameters of ZnO Nanoparticles Using Various Peak Profile Analysis

Abstract

Publication series

Bibliographical note

Keywords

ASJC Scopus subject areas

Access to Document

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