Comparison of dry, wet and microwave digestion methods for the multi element determination in some dried fruit samples by ICP-OES

  • Huseyin Altundag*
  • , Mustafa Tuzen
  • *Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

160 Scopus citations

Abstract

The aim of this study was used to investigate the level of trace metals (Ba, Pb, Cd, Mn, Cr, Co, Ni, Cu, Mn, Zn, Sr and Fe) in some dried fruits (Prunus domestica L., Ficus carica L., Morus alba L., Vitis vinifera L., Prunus armeniaca L., and Malus domestica) samples from Turkey. Trace elements were determined by ICP-OES after dry, wet and microwave digestion methods in dried fruit samples. Validation of the proposed method was carried out by using a NIST-SRM 1515-Apple Leaves certified reference material. Element concentrations in dried fruit samples were 0.33-1.77 (Ba), 0.12-0.54 (Cd), 0.25-1.03 (Co), 0.45-2.30 (Cr), 0.43-2.74 (Cu), 0.56-4.87 (Mn), 0.61-2.54 (Ni), 0.40-2.14 (Pb), 2.16-6.54 (Zn), 0.83-12.02 (Al), 11.82-40.80 (Fe) and 0.16-6.34 (Sr) μg/g. The analytical parameters show that the microwave oven digestion procedure provided best results as compared to the wet and dry digestion procedures. The results were compared with the literature values.

Original languageEnglish
Pages (from-to)2800-2807
Number of pages8
JournalFood and Chemical Toxicology
Volume49
Issue number11
DOIs
StatePublished - Nov 2011
Externally publishedYes

Bibliographical note

Funding Information:
This work was supported partly by Sakarya University Scientific Research Foundation with Project Number 2010-02-04-015.

Keywords

  • Dried fruit
  • Dry ashing
  • ICP-OES
  • Microwave digestion
  • Trace element
  • Wet ashing

ASJC Scopus subject areas

  • Food Science
  • Toxicology

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