Column solid-phase extraction of nickel and silver in environmental samples prior to their flame atomic absorption spectrometric determinations

Mustafa Tuzen; Mustafa Soylak

doi:10.1016/j.jhazmat.2008.09.050

Column solid-phase extraction of nickel and silver in environmental samples prior to their flame atomic absorption spectrometric determinations

Mustafa Tuzen
, Mustafa Soylak^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

128 Scopus citations

Abstract

A biosorption procedure for preconcentration-separation of nickel(II) and silver(I) at trace levels on Bacillus sphaericus-loaded Chromosorb 106 (BSLC106) has been presented in this work. The conditions like pH, amounts of microorganism, eluent type, etc. for the quantitative adsorption of the analyte ions on BSCL106 column were investigated. The analyte ions were quantitatively recovered and desorbed at pH range of 6.0-7.0 and 10 mL of 1 M HCl, respectively. The effects of various cationic and anionic interferences on the recoveries of nickel(II) and silver(I) were studied. The detection limits for nickel(II) and silver(I) are 1.42 and 1.05 μg L^-1, respectively. The accuracy of the developed procedure was tested by analyzing NIST SRM 2711 Montana soil and GBW 07310 Stream sediment certified reference materials. The proposed enrichment-separation procedure was successfully applied to the determination of analytes in natural water, black tea, tobacco, soil and sediment samples with satisfactory results.

Original language	English
Pages (from-to)	1428-1432
Number of pages	5
Journal	Journal of Hazardous Materials
Volume	164
Issue number	2-3
DOIs	https://doi.org/10.1016/j.jhazmat.2008.09.050
State	Published - 30 May 2009
Externally published	Yes

Bibliographical note

Funding Information:
The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank Dr. Canan Usta for the preparation of microorganism and the Scientific and Technological Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163).

Keywords

Atomic absorption spectrometry
Bacillus sphaericus
Chromosorb 106
Nickel(II)
Preconcentration
Silver(I)

ASJC Scopus subject areas

Environmental Engineering
Environmental Chemistry
Waste Management and Disposal
Pollution
Health, Toxicology and Mutagenesis

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10.1016/j.jhazmat.2008.09.050

Cite this

@article{98122d55599342bd9310e4ca3e863837,

title = "Column solid-phase extraction of nickel and silver in environmental samples prior to their flame atomic absorption spectrometric determinations",

abstract = "A biosorption procedure for preconcentration-separation of nickel(II) and silver(I) at trace levels on Bacillus sphaericus-loaded Chromosorb 106 (BSLC106) has been presented in this work. The conditions like pH, amounts of microorganism, eluent type, etc. for the quantitative adsorption of the analyte ions on BSCL106 column were investigated. The analyte ions were quantitatively recovered and desorbed at pH range of 6.0-7.0 and 10 mL of 1 M HCl, respectively. The effects of various cationic and anionic interferences on the recoveries of nickel(II) and silver(I) were studied. The detection limits for nickel(II) and silver(I) are 1.42 and 1.05 μg L-1, respectively. The accuracy of the developed procedure was tested by analyzing NIST SRM 2711 Montana soil and GBW 07310 Stream sediment certified reference materials. The proposed enrichment-separation procedure was successfully applied to the determination of analytes in natural water, black tea, tobacco, soil and sediment samples with satisfactory results.",

keywords = "Atomic absorption spectrometry, Bacillus sphaericus, Chromosorb 106, Nickel(II), Preconcentration, Silver(I)",

author = "Mustafa Tuzen and Mustafa Soylak",

note = "Funding Information: The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank Dr. Canan Usta for the preparation of microorganism and the Scientific and Technological Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163).",

year = "2009",

month = may,

day = "30",

doi = "10.1016/j.jhazmat.2008.09.050",

language = "English",

volume = "164",

pages = "1428--1432",

journal = "Journal of Hazardous Materials",

issn = "0304-3894",

publisher = "Elsevier BV",

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TY - JOUR

T1 - Column solid-phase extraction of nickel and silver in environmental samples prior to their flame atomic absorption spectrometric determinations

AU - Tuzen, Mustafa

AU - Soylak, Mustafa

N1 - Funding Information: The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank Dr. Canan Usta for the preparation of microorganism and the Scientific and Technological Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163).

PY - 2009/5/30

Y1 - 2009/5/30

N2 - A biosorption procedure for preconcentration-separation of nickel(II) and silver(I) at trace levels on Bacillus sphaericus-loaded Chromosorb 106 (BSLC106) has been presented in this work. The conditions like pH, amounts of microorganism, eluent type, etc. for the quantitative adsorption of the analyte ions on BSCL106 column were investigated. The analyte ions were quantitatively recovered and desorbed at pH range of 6.0-7.0 and 10 mL of 1 M HCl, respectively. The effects of various cationic and anionic interferences on the recoveries of nickel(II) and silver(I) were studied. The detection limits for nickel(II) and silver(I) are 1.42 and 1.05 μg L-1, respectively. The accuracy of the developed procedure was tested by analyzing NIST SRM 2711 Montana soil and GBW 07310 Stream sediment certified reference materials. The proposed enrichment-separation procedure was successfully applied to the determination of analytes in natural water, black tea, tobacco, soil and sediment samples with satisfactory results.

AB - A biosorption procedure for preconcentration-separation of nickel(II) and silver(I) at trace levels on Bacillus sphaericus-loaded Chromosorb 106 (BSLC106) has been presented in this work. The conditions like pH, amounts of microorganism, eluent type, etc. for the quantitative adsorption of the analyte ions on BSCL106 column were investigated. The analyte ions were quantitatively recovered and desorbed at pH range of 6.0-7.0 and 10 mL of 1 M HCl, respectively. The effects of various cationic and anionic interferences on the recoveries of nickel(II) and silver(I) were studied. The detection limits for nickel(II) and silver(I) are 1.42 and 1.05 μg L-1, respectively. The accuracy of the developed procedure was tested by analyzing NIST SRM 2711 Montana soil and GBW 07310 Stream sediment certified reference materials. The proposed enrichment-separation procedure was successfully applied to the determination of analytes in natural water, black tea, tobacco, soil and sediment samples with satisfactory results.

KW - Atomic absorption spectrometry

KW - Bacillus sphaericus

KW - Chromosorb 106

KW - Nickel(II)

KW - Preconcentration

KW - Silver(I)

UR - https://www.scopus.com/pages/publications/62649102754

U2 - 10.1016/j.jhazmat.2008.09.050

DO - 10.1016/j.jhazmat.2008.09.050

M3 - Article

C2 - 18977595

AN - SCOPUS:62649102754

SN - 0304-3894

VL - 164

SP - 1428

EP - 1432

JO - Journal of Hazardous Materials

JF - Journal of Hazardous Materials

IS - 2-3

ER -

Column solid-phase extraction of nickel and silver in environmental samples prior to their flame atomic absorption spectrometric determinations

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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