Aluminium determination in environmental samples by graphite furnace atomic absorption spectrometry after solid phase extraction on Amberlite XAD-1180/pyrocatechol violet chelating resin

Ibrahim Narin; Mustafa Tuzen; Mustafa Soylak

doi:10.1016/j.talanta.2003.11.005

Aluminium determination in environmental samples by graphite furnace atomic absorption spectrometry after solid phase extraction on Amberlite XAD-1180/pyrocatechol violet chelating resin

Ibrahim Narin
, Mustafa Tuzen
, Mustafa Soylak^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

179 Scopus citations

Abstract

A chelating resin, pyrocatechol violet (PV) immobilised on an Amberlite XAD-1180 support, was prepared and its use for the atomic absorption spectrometric determination of aluminium was investigated. The XAD-1180-PV resin was characterised by infrared spectrometry and thermal gravimetric analysis. The optimum pH value for quantitative sorption is 8-9, and desorption can be achieved by using 5.0-10.0 ml of 2 M HCl. The effects of diverse ions on the sorption and recovery of aluminium have been studied. The capacity of sorbent was 6.45±0.59 mg g^-1 Al XAD-1180-PV. Recoveries for aluminium from water samples were in the range 95-105%. The accuracy of procedure was confirmed by aluminium determination in certified reference materials. The method developed was applied with varying results to the analysis of natural water, haemodialysis fluids and microwave digested red wine samples from Tokat City.

Original language	English
Pages (from-to)	411-418
Number of pages	8
Journal	Talanta
Volume	63
Issue number	2
DOIs	https://doi.org/10.1016/j.talanta.2003.11.005
State	Published - 28 May 2004
Externally published	Yes

Bibliographical note

Funding Information:
The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank the Scientific and Technical Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163). Also the authors thank to Pamukkale University Fen Edebiyat Faculty for thermogravimetric analysis.

Keywords

AAS
Amberlite XAD-1180
Chelating resin
Preconcentration
Pyrocatechol violet

ASJC Scopus subject areas

Analytical Chemistry

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10.1016/j.talanta.2003.11.005

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title = "Aluminium determination in environmental samples by graphite furnace atomic absorption spectrometry after solid phase extraction on Amberlite XAD-1180/pyrocatechol violet chelating resin",

abstract = "A chelating resin, pyrocatechol violet (PV) immobilised on an Amberlite XAD-1180 support, was prepared and its use for the atomic absorption spectrometric determination of aluminium was investigated. The XAD-1180-PV resin was characterised by infrared spectrometry and thermal gravimetric analysis. The optimum pH value for quantitative sorption is 8-9, and desorption can be achieved by using 5.0-10.0 ml of 2 M HCl. The effects of diverse ions on the sorption and recovery of aluminium have been studied. The capacity of sorbent was 6.45±0.59 mg g-1 Al XAD-1180-PV. Recoveries for aluminium from water samples were in the range 95-105\%. The accuracy of procedure was confirmed by aluminium determination in certified reference materials. The method developed was applied with varying results to the analysis of natural water, haemodialysis fluids and microwave digested red wine samples from Tokat City.",

keywords = "AAS, Amberlite XAD-1180, Chelating resin, Preconcentration, Pyrocatechol violet",

author = "Ibrahim Narin and Mustafa Tuzen and Mustafa Soylak",

note = "Funding Information: The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank the Scientific and Technical Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163). Also the authors thank to Pamukkale University Fen Edebiyat Faculty for thermogravimetric analysis.",

year = "2004",

month = may,

day = "28",

doi = "10.1016/j.talanta.2003.11.005",

language = "English",

volume = "63",

pages = "411--418",

journal = "Talanta",

issn = "0039-9140",

publisher = "Elsevier BV",

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TY - JOUR

T1 - Aluminium determination in environmental samples by graphite furnace atomic absorption spectrometry after solid phase extraction on Amberlite XAD-1180/pyrocatechol violet chelating resin

AU - Narin, Ibrahim

AU - Tuzen, Mustafa

AU - Soylak, Mustafa

N1 - Funding Information: The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Gaziosmanpasa University and the Unit of the Scientific Research Projects of Erciyes University. The authors also would like to thank the Scientific and Technical Research Council of Turkey (TUBITAK) for financial helps (TBAG 2163). Also the authors thank to Pamukkale University Fen Edebiyat Faculty for thermogravimetric analysis.

PY - 2004/5/28

Y1 - 2004/5/28

N2 - A chelating resin, pyrocatechol violet (PV) immobilised on an Amberlite XAD-1180 support, was prepared and its use for the atomic absorption spectrometric determination of aluminium was investigated. The XAD-1180-PV resin was characterised by infrared spectrometry and thermal gravimetric analysis. The optimum pH value for quantitative sorption is 8-9, and desorption can be achieved by using 5.0-10.0 ml of 2 M HCl. The effects of diverse ions on the sorption and recovery of aluminium have been studied. The capacity of sorbent was 6.45±0.59 mg g-1 Al XAD-1180-PV. Recoveries for aluminium from water samples were in the range 95-105%. The accuracy of procedure was confirmed by aluminium determination in certified reference materials. The method developed was applied with varying results to the analysis of natural water, haemodialysis fluids and microwave digested red wine samples from Tokat City.

AB - A chelating resin, pyrocatechol violet (PV) immobilised on an Amberlite XAD-1180 support, was prepared and its use for the atomic absorption spectrometric determination of aluminium was investigated. The XAD-1180-PV resin was characterised by infrared spectrometry and thermal gravimetric analysis. The optimum pH value for quantitative sorption is 8-9, and desorption can be achieved by using 5.0-10.0 ml of 2 M HCl. The effects of diverse ions on the sorption and recovery of aluminium have been studied. The capacity of sorbent was 6.45±0.59 mg g-1 Al XAD-1180-PV. Recoveries for aluminium from water samples were in the range 95-105%. The accuracy of procedure was confirmed by aluminium determination in certified reference materials. The method developed was applied with varying results to the analysis of natural water, haemodialysis fluids and microwave digested red wine samples from Tokat City.

KW - AAS

KW - Amberlite XAD-1180

KW - Chelating resin

KW - Preconcentration

KW - Pyrocatechol violet

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DO - 10.1016/j.talanta.2003.11.005

M3 - Article

AN - SCOPUS:2142765895

SN - 0039-9140

VL - 63

SP - 411

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JO - Talanta

JF - Talanta

IS - 2

ER -

Aluminium determination in environmental samples by graphite furnace atomic absorption spectrometry after solid phase extraction on Amberlite XAD-1180/pyrocatechol violet chelating resin

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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