A Taguchi approach to synthesise Al/Fe core–shell composite powders through electroless deposition

Rashid Ali, Fahad Ali*, Aqib Zahoor, Rub Nawaz Shahid, Naeem ul Haq Tariq, Saad Ullah, Rizwan Ahmed, Hasan Bin Awais

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

3 Scopus citations

Abstract

In the present study, Al/Fe core–shell particles were successfully synthesised by electroless deposition of iron on aluminium particles. The process variables were investigated and optimised to achieve maximum deposition efficiency. These variables, including chemical composition parameters (molar ratios of salt/reducing agent, salt/complexing agent and pH) and process parameters (particle size, temperature and time) were optimised by using the Taguchi method. The chemical composition of iron deposited aluminium particles, their morphology and coating quality were characterised by helium gas pycnometry, scanning electron microscopy, energy-dispersive spectroscopy and X-ray diffraction. The results revealed that, by using the optimised bath chemical composition and optimised process parameters, a maximum of 28.91% iron deposition on aluminium particles can be obtained within 20 min.

Original languageEnglish
Pages (from-to)265-273
Number of pages9
JournalTransactions of the Institute of Metal Finishing
Volume99
Issue number5
DOIs
StatePublished - 2021
Externally publishedYes

Bibliographical note

Publisher Copyright:
© 2021 Institute of Materials Finishing Published by Taylor & Francis on behalf of the Institute.

Keywords

  • Al/Fe composite powder
  • ANOVA
  • Core–shell particles
  • electroless deposition
  • interaction of coating parameters
  • iron deposition
  • optimal parameters
  • Taguchi method

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Mechanics of Materials
  • Surfaces and Interfaces
  • Surfaces, Coatings and Films
  • Metals and Alloys

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