A Novel Selective Deep Eutectic Solvent Extraction Method for Versatile Determination of Copper in Sediment Samples by ICP-OES

Esra Bağda; Huseyin Altundağ; Mustafa Tüzen; Mustafa Soylak

doi:10.1007/s00128-017-2065-y

A Novel Selective Deep Eutectic Solvent Extraction Method for Versatile Determination of Copper in Sediment Samples by ICP-OES

Esra Bağda^*
, Huseyin Altundağ
, Mustafa Tüzen
, Mustafa Soylak

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

42 Scopus citations

Abstract

In the present study, a simple, mono step deep eutectic solvent (DES) extraction was developed for selective extraction of copper from sediment samples. The optimization of all experimental parameters, e.g. DES type, sample/DES ratio, contact time and temperature were performed with using BCR-280 R (lake sediment certified reference material). The limit of detection (LOD) and the limit of quantification (LOQ) were found as 1.2 and 3.97 µg L⁻¹, respectively. The RSD of the procedure was 7.5%. The proposed extraction method was applied to river and lake sediments sampled from Serpincik, Çeltek, Kızılırmak (Fadl and Tecer region of the river), Sivas-Turkey.

Original language	English
Pages (from-to)	264-269
Number of pages	6
Journal	Bulletin of Environmental Contamination and Toxicology
Volume	99
Issue number	2
DOIs	https://doi.org/10.1007/s00128-017-2065-y
State	Published - Aug 2017
Externally published	Yes

Bibliographical note

Publisher Copyright:
© 2017, Springer Science+Business Media New York.

Keywords

Deep eutectic solvent
Extraction
Inductively coupled plasma optical emission spectrometry
Sediment

ASJC Scopus subject areas

Toxicology
Pollution
Health, Toxicology and Mutagenesis

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10.1007/s00128-017-2065-y

Cite this

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abstract = "In the present study, a simple, mono step deep eutectic solvent (DES) extraction was developed for selective extraction of copper from sediment samples. The optimization of all experimental parameters, e.g. DES type, sample/DES ratio, contact time and temperature were performed with using BCR-280 R (lake sediment certified reference material). The limit of detection (LOD) and the limit of quantification (LOQ) were found as 1.2 and 3.97 µg L−1, respectively. The RSD of the procedure was 7.5\%. The proposed extraction method was applied to river and lake sediments sampled from Serpincik, {\c C}eltek, Kızılırmak (Fadl and Tecer region of the river), Sivas-Turkey.",

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author = "Esra Bağda and Huseyin Altundağ and Mustafa T{\"u}zen and Mustafa Soylak",

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month = aug,

doi = "10.1007/s00128-017-2065-y",

language = "English",

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T1 - A Novel Selective Deep Eutectic Solvent Extraction Method for Versatile Determination of Copper in Sediment Samples by ICP-OES

AU - Bağda, Esra

AU - Altundağ, Huseyin

AU - Tüzen, Mustafa

AU - Soylak, Mustafa

PY - 2017/8

Y1 - 2017/8

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AB - In the present study, a simple, mono step deep eutectic solvent (DES) extraction was developed for selective extraction of copper from sediment samples. The optimization of all experimental parameters, e.g. DES type, sample/DES ratio, contact time and temperature were performed with using BCR-280 R (lake sediment certified reference material). The limit of detection (LOD) and the limit of quantification (LOQ) were found as 1.2 and 3.97 µg L−1, respectively. The RSD of the procedure was 7.5%. The proposed extraction method was applied to river and lake sediments sampled from Serpincik, Çeltek, Kızılırmak (Fadl and Tecer region of the river), Sivas-Turkey.

KW - Deep eutectic solvent

KW - Extraction

KW - Inductively coupled plasma optical emission spectrometry

KW - Sediment

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U2 - 10.1007/s00128-017-2065-y

DO - 10.1007/s00128-017-2065-y

M3 - Article

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AN - SCOPUS:85015616027

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IS - 2

ER -

A Novel Selective Deep Eutectic Solvent Extraction Method for Versatile Determination of Copper in Sediment Samples by ICP-OES

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

Access to Document

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